Influence of layer thickness and heat treatment on microstructure and properties of selective laser melted maraging stainless steel

Abstract

As one of the main parameters of selective laser melting (SLM) process, layer thickness has a significant impact on the forming performance and efficiency of printed parts. Based on microstructure analysis and properties testing, the metallurgical mechanism, phase composition and mechanical behavior of SLM-formed Corrax stainless steel with different layer thicknesses were discussed. The influence of heat treatment process on the properties was comparatively investigated. The results indicated that at smaller or larger layer thicknesses, the increase in melt dynamic instability and spheroidisation feature easily induced the formation of unfused pore defects, which in turn led to lower relative density and mechanical properties. At the appropriate layer thickness, the suitable melt flow behaviour promoted the formation of good metallurgical bonding between adjacent melt channels. The maximum tensile strength, yield strength and hardness of the samples prepared at a layer thickness of 60 μm were 1224 MPa, 948 MPa and 39.2 HRC, respectively. The microstructure of the as-built samples was martensite and a small amount of austenite. With increasing layer thickness, the cooling rate of the molten pool decreased and the austenite content increased. After solution treatment, the alloying elements dissolved in the martensitic matrix resulted in lower mechanical properties. After aging and solution aging treatment, the mechanical properties were significantly improved due to precipitation strengthening of NiAl nanoparticles and dislocation strengthening. The corresponding tensile strengths were 1655 MPa and 1796 MPa, the yield strengths were 1328 MPa and 1573 MPa, and the hardnesses were 45.7 HRC and 50.2 HRC, respectively.