Influence of initial solid–liquid interface morphology on further microstructure evolution during directional solidification

Abstract

Preparation of the initial solid–liquid interface on which growth is started is a very critical step in directional solidification experiments. Dedicated experiments concerning preparation of the initial solid–liquid interface morphology and its influence on further directionally solidified microstructure were performed on Cu-20 wt% Sn peritectic alloy in a Bridgman-type furnace. To verify the morphology of the initial solid–liquid interface, steady-state directional dendritic growth was interrupted by thermal stabilization ranging from 0 to 1 h prior to quenching. With thermal stabilization duration increase, the solid–liquid interface morphology degenerated from dendritic to cellular and finally to planar. To verify the influence of the initial state on further solidification microstructure, directional solidification experiments were performed at a low pulling rate of 1 μm/s with different initial solid–liquid interface morphologies. The initial state affects solute redistribution and formation of peritectic coupled growth structure in the subsequent directional solidification process.