Abstract
A composite with a high-alloy steel matrix was reinforced with varying amounts of Mg-PSZ and synthesized using Spark Plasma Sintering (SPS) technology. To prepare the powders for sintering, they were mixed in a planetary ball mill at two different rates of 100 rpm and 250 rpm. The influence of the rotation speed on the microstructures and compressive strengths of the sintered composites was investigated. Due to the high degree of deformation of the steel powder particles during milling at 250 rpm, the steel phase underwent grain refinement during SPS. Furthermore, the Mg-PSZ was more homogeneously distributed within the steel matrix and mechanically interlocked with the steel matrix. Thus, the compressive strength of the composite increased with increasing Mg-PSZ content and increasing rotation speed during milling of the powder due to grain refinement and the improved strength of the steel/ceramic interface. Furthermore, a larger amount of Mg-PSZ underwent stress-induced transformation under compressive loading.
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