Abstract
In this work samples of Fe-Mn alloys were subjected to equal-channel angular pressing (ECAP) in order to study the effect of the resulting microstructure on the mechanical properties, biodegradation rate, and biocompatibility in vitro of the alloys. The microstructure of the alloys was studied by scanning and transmission electron microscopy, as well as by X-ray diffraction analysis. Mechanical properties were studied by microhardness and tensile tests. It is shown that as a result of deformation by the ECAP method, a predominantly austenitic ultrafine-grained (UFG) structure is formed, shear bands up to 600 nm thick and nanosized twins up to 40 nm thick were observed. The release of α-Mn particles in the ECAP process was revealed. Due to the structure refinement and twinning during ECAP, the strength characteristics of Fe-Mn alloys were significantly increased compared to the corresponding alloys in the initial annealed state. An increase in the propensity to biodegradation of UFG alloys with their satisfactory hemocompatibility was observed.
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