Abstract
The effect of minor Al addition on structural, crystallization, soft magnetic behaviour and magnetic field induced anisotropy through DC Joule annealing in (Fe53.95Co29.05)83Si1.3B11.7-xNb3Cu1Alx, (X=0, 1) alloys has been studied. The Al added as-quenched melt spun ribbons show good glass forming ability, better thermo-physical properties like a high Tx1 of 438°C, Tcam of 435°C and Tcnc of 906°C, compared to Tx1 of 389°C, Tcam of 409°C and Tcnc of 900°C for the alloy without Al addition. The longitudinal magnetic field annealed Al added alloy exhibits low Hc of 12.92A/m and maximum Ms. of 1.78T. The better soft magnetic properties of Al added alloy are achieved through a high nucleation density of BCC-FeCo(Al) nanocrystallites having low K1 and λ values. The as-quenched alloys possess high magneto-strain exceeding 30ppm and approach near zero value on nanocrystallization. The longitudinal magnetic field assisted DC Joule annealing, having current density (J) in the range of J=20–25A/mm2 promotes good magnetic softening due to precipitation of 5–35nm nanocrystallites as explained by extended-random anisotropy model. The Al added alloy shows better magnetic field induced anisotropy (Ku) on nanocrystallization and shows visible change in the shape of hysteresis loop.
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