Influence of adding Ti powder in preform on microstructure and mechanical properties of Al2O3p/steel composites by squeeze casting

Abstract

To improve the mechanical properties of alumina particulates reinforced steel matrix composite, Ti powder was added into the alumina preform, a 5140 steel matrix composite was fabricated by squeeze casting, and the influences of Ti powder on the microstructure, hardness and bending strength of the composite were investigated, compared with the composite without adding Ti powder. Applied Ti powder and alumina particulates were 10-25 μm and 100-180 μm in size, respectively. Both composites were successfully fabricated, however Ti powder addition increased the infiltration thickness of the composite. In the Ti contained composite, a TiC film in micron scale is formed on the surface of alumina particles, many TiC aggregates are dispersed in the steel matrix without obvious remaining Ti powder. The hardness and the three-point bending strength of the composite reach 49.5 HRC and 1 018 MPa, respectively, which are 17.9% and 52.4% higher than those of the composite in the absence of Ti addition. Fracture morphology shows that the debonding of alumina particulates is eliminated for the composite in the presence of Ti addition. Sessile drop test shows the average wetting angle between 5140 steel and that of Ti coated Al2O3 is about 82.15°, much lower than the wetting angle 150° between steel and pure Al2O3. Therefore, the increase in the mechanical properties of the composite is attributed to the improvement of Al2O3p/steel interface wetting and bonding by adding Ti powder in the preform.