Abstract
Indirectly detected, through-bond NMR correlation spectra between 13C and 1H nuclei are reported for the first time in solid state. The capabilities of the new method are demonstrated using naturally abundant organic–inorganic mesoporous hybrid materials. The time performance is significantly better, almost by a factor of 10, than in the corresponding 13C detected experiment. The proposed scheme represents a new analytical tool for studying other solid-state systems and the basis for the development of more advanced 2D and 3D correlation methods.
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