Abstract

An effective and economically viable vertical semi transparent Bridgman setup has been designed and fabricated by employing a furnace made up of a single Nichrome coil. We made an effort with a new approach by adapting a translation mechanism for the ampoule coupled with a stop clock. This set up is a suitable device for growing organic crystal from melt as it makes use of ampoule translation assembly. Organic nonlinear materials of acenaphthene and benzophenone were grown using this set up. Transparent single crystals were successfully grown as a result of suitable thermal gradient achieved by means of thermal gradient furnace assembly. The grown single crystals were rationalized using X-ray diffraction, spectroscopic and thermal analysis.

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