Abstract
The evolution of the structural phases of the Fe-42.4 at% Ga alloy was studied using neutron diffraction performed with high-intensity continuous scanning in a wide temperature range. The sequence of occurrence of structural states both during heating and subsequent cooling is reported. The structural phases Fe13Ga13, Fe13Ga9, α-Fe6Ga5, D03, L12, A2 are present in the alloy and they disappear upon heating above 800 °C into the partially ordered B2/A2 phase. The high-temperature Fe13Ga13 intermetallic compound exists in two temperature ranges: 25–580 °С and 770–800 °С during heating and precipitates again during cooling. The persistence of the phase upon cooling down to room temperature is inconsistent with the phase diagram, indicating that the alloy remains in a metastable state after the heating and subsequent cooling. The D03, α-Fe6Ga5 and L12 phases are formed during cooling.
Published Version
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