Abstract
Deciphering <i>in situ</i> structure of layer double hydroxides (LDHs) and their corresponding mechanism of oxygen evolution reaction (OER) is essential to further development of LDH-based OER catalysts. In this issue of <i>Chem Catalysis</i>, Ko et al. demonstrated a scalable synthesis of ultrathin Ni-Fe LDH nanostructure, its chemical oxidation process, and its catalytic mechanism by <i>in situ/operando</i> spectroscopies, paving a solid pathway to potential practical application of LDH-based catalysts.
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