Abstract

In situ XPS analysis of the electrochemical system [EMIM][BF 4]/Pt was performed in a three electrode electrochemical cell as a function of electrode potential. The so-called electrochemical shift of the binding energy of electrolyte species with the applied electrode potential is confirmed. The reductive degradation of [EMIM][BF 4] at a potential of − 1.9 V vs. a carbon quasi reference electrode is demonstrated.

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