In Situ Electrical Resistance Measurement of Pure Titanium During Severe Plastic Deformation by High‐Pressure Sliding

Abstract

In this study, in situ measurements of electrical resistance in pure Ti during severe plastic deformation (SPD) under high pressures are presented. The process of high‐pressure sliding (HPS) is adopted for the SPD so that straining is feasible under various pressures covering α to ω allotropic phase transformation in pure Ti. Anvil surfaces are coated by a plasma‐sprayed alumina layer to maintain electrical insulation between the sample and the anvils during HPS operation. The electrical resistance increases continuously with straining by the HPS processing but the increase in the electrical resistance is more pronounced as the applied pressure increases, particularly when the ω phase formation occurs. The phase transformation is evidenced by X‐Ray diffraction analysis as well as in situ static heating experiment. The continuous increase in the electrical resistance suggests that there is neither critical strain nor avalanche for the phase transformation to the ω phase.