Abstract
Cyanuric fluoride (2) is one of the most popular fluorinating agents in organic chemistry. The title compound could be prepared in a 50 to 100 g scale by means of a chlorine fluorine exchange, the process was characterized by a simple preparation procedure, cheap reactants and a low time exposure. Carboxylic acids were converted into the corresponding acid fluorides 4a-g using cyanuric fluoride. A non-aqueous work-up led to high yields on synthesizing a range of functionalized acid fluorides.
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