Abstract
A new pressure‐free synthesis method was developed producing the porous material Cu3(BTC)2 (BTC = benzene tricarboxylate) with a very high micropore volume up to 0.62 cm3g–1. The compound is a promising nanoporous solid for adsorptive hydrogen storage under cryogenic conditions with a capacity of 2.18 wt% which is higher than that of IRMOFs and other coordination polymers.
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