Identification of wetting and molecular diffusion stages during self-healing process of asphalt binder via fluorescence microscope

Abstract

In order to distinguish the wetting healing stage and the molecular diffusion healing stage during the self-healing process of asphalt binders, the fluorescence microscope (FM) together with the image processing technique was employed. The healing index was put forward based on the variation of crack area. On the basis of the established capillary diffusion theory, the Two-Stage Model was built to fit the healing curves characterizing the healing index variation with healing time. It is found that the established method is quite suitable to identify the wetting and the diffusion stages. The wetting healing occurs firstly, during which the asphalt molecules spontaneously wet the both faces of crack. Although the strength recovery is not distinct at this stage, SBS modified asphalt shows greater wetting healing strength than the other neat asphalt binders. Once the wetting process is nearly finished, the molecular diffusion healing ratio accelerates significantly, and the descending order of the molecular diffusion rate is: SBS>PEN 100>PEN 70>PEN 50>PEN 20. The test results also show that the disappearance of visible crack does not indicate that the strength has been fully recovered. Here, the tensile strength test is developed to identify the strength recovery rate after the crack is fully closed, which implies that the strength regeneration is a long process.