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Abstract
Abstract Various intermediates of mononuclear copper(II) cyanide complexes in the reaction of cupric ions with cyanide ions have been first identified by ESR spectroscopy after the use of a newly-constructed rapid-freezing apparatus. The formation of these intermediates has been found to depend primarily on the ratio [CN−]/[Cu2+] and pH values. Possible structures of these intermediate complexes have been estimated by experiments with isotopes and by the application of the “rule of average environment” to their ESR parameters determined.
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