Abstract
<p>The synthesis and characterization of M-MCM-48 (M= Si, Ti, V, Cr and Mn) materials have been carried out. These systems promote hydroxylation of phenol with 30 % H<sub>2</sub>O<sub>2</sub> and the hydroxylation activity is highest for Ti-MCM-48. Water appears to be a better solvent than acetone and acetonitrile.</p>
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