Abstract
Hydrothermal syntheses of nano- and microparticles of metal oxides of two types, LiMOn (LiCoO2, LiNiO2, LiZnO2, and LiCuO2) and MOn (Ga2O3, CeO2) were performed under continuous conditions in a tubular reactor with the use of supercritical water. An important role in the synthesis of nanoparticles and the reproducibility of the results was played by the conditions of mixing of supercritical water and precursor solution flows. The morphology and composition of synthesized compounds were studied by scanning electron microscopy and X-ray diffraction. The syntheses of LiCoO2, LiNiO2, LiZnO2, LiCuO2, Ga2O3, and CeO2 were most successful.
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