Abstract

AbstractThis study presents the synthesis and characterization of Copper Oxide/Tungsten Oxide (CuO/WO3) hybrid bifunctional composites using a hydrothermal approach. X‐ray diffraction (XRD) analysis confirms the successful synthesis of CuO/WO3 hybrids, exhibiting additional peaks corresponding to WO3 phases. Scanning electron microscopy (SEM) images reveal well‐defined, aggregated particles with a nanoscale pattern and uniform distribution of CuO and WO3 throughout the composite. Energy‐dispersive X‐ray spectroscopy (EDX) confirms the stoichiometric composition of CuO/WO3 hybrids. Evaluation of dark adsorption and sunlight‐assisted photocatalysis using methylene blue (MB) dyes shows a remarkable enhancement in efficiency compared to pristine CuO. The CuO/WO3 hybrids exhibit a dark adsorption capacity of 87 % and a photocatalytic degradation efficiency of 95 % under sunlight illumination, outperforming pure CuO. These results underscore the synergistic interaction between CuO and WO3, facilitating efficient pollutant removal. The study elucidates the structural properties and mechanistic insights driving the superior performance of CuO/WO3 hybrid composites, offering promising prospects for advanced water treatment technologies.

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