Abstract
A novel three-dimensional (3D) supramolecular assembly of Standberg-type polyoxometalate and flexible organic molecule (H2bpp)3[Mo5P2O23]·H2O (1) [bpp = 1,3-bis(4-pyridyl)propane] has been hydrothermally synthesized and structurally characterized by single-crystal X-ray diffraction, IR spectra, elemental analysis and thermogravimetric analysis (TGA). X-ray analyses show that compound 1 represent a twofold interpenetrating 3D supramolecular architecture constructed of Standberg-type polyoxometalate and bpp molecular through the hydrogen bonds as well as electrostatic interactions.
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