Abstract
The new complexes {[Co2(BPPA)(hfipbb)2(H2O)(DMF)2](H2O)4}n and {[Ni2(BPPA)(hfipbb)2(H2O)(DMF)2](H2O)4}n have been synthesized under solvothermal conditions. These isostructural complexes exhibit 2D bilayer networks with unprecedented {411.64} topology.
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