Abstract
X-ray structural data are reported for tetraethylammonium-2-hydroxythiobenzoate (C15H25NO2S; orthorhombic,Pna21(33);a=14.155(2)A,b=7.651(1)A,c=14.855(2)A;Z=4;R=0.038, at 295 K) and for tetraethylammonium-2-hydroxydithiobenzoate (C15H25NOS2; orthorhombic,Pna21(33);a=15.668(4)A,b=8.729(2)A,c=12.350(3)A;Z=4;R=0.031, at 295 K). In both compounds the OH groups are engaged in intramolecular O-H⋯S hydrogen bonds (O⋯S=2.88 and 2.89 A, respectively).
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