Abstract
A general and simple preparative method for the synthesis of α-hydroxyalky(benzyl)furazan and -furoxan derivatives is proposed, The method involves reduction of acyl or ethoxycarbonyl substituents in these heterocyclic compounds with NaBH4 in ethanol. Based on the alcohols thus prepared, a number of previously unknown functional derivatives (α-nitroxyalkyl-α-haloalkyl-, and α-azidoalkylfurazans and -furoxans) have been synthesized.
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