Abstract
Hydroalumination-iodinolysis of 3-butyn-1-ol ( 2) provided E-4-iodo-3-buten-1-ol (4E) as the major product. This compound was transformed in three steps into the leaf roller moth sex pheromone 1 with high (>99% de) stereoselectivity and good overall yield (4 steps, 39% from 2).
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