HPLC-FLD determination of aflatoxins M1 and M2 in raw cow milk samples using in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method

Abstract

An in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method was employed for the extraction of aflatoxins from cow milk samples prior to their quantification with HPLC equipped with a fluorescence detector.