Abstract
Zeolite-encapsulated ruthenium(III) salophen (ZERS) was prepared by flexible ligand method and characterized by diffuse reflectance FT-IR and UV–vis spectroscopic methods, X-ray diffraction, BET, SEM, TEM and elemental analysis. The amount of Ru-salophen in the zeolite supercages was 0.018mmol/g of encapsulated zeolite. This catalyst was used for efficient and selective epoxidation of different alkenes with NaIO4 under magnetic stirring and ultrasonic irradiation conditions. This catalyst also showed a good shape-selectivity in the epoxidation of linear alkenes. This heterogeneous catalyst was reused several times without significant loss of its catalytic activity.
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