Abstract

Abstract. Nuclear magnetic resonance (NMR) experiments are usually carried out at very high and homogenous magnetic fields. However, portable systems have emerged in recent years at low fields, offering many advantages like easier maintenance and open design that permit us to imagine a variety of coil configurations in order to maximize the homogeneity of the static field B0 and the radio-frequency field B1. The wire winding distribution based on space harmonics suppression (SHS) of the cosine current density distribution offers new possibilities of producing homogenous static fields B0. In this work, an extension of the SHS method, allowing homogeneity enhancement and flexibility of the coil design, is presented. The efficiency of the method is demonstrated through the construction of homogenous magnetic field coils dedicated to a very low magnetic field (8 mT) 1H NMR spectrometer. The performance of these coils in terms of magnetic field intensity and homogeneity as well as self-heating behavior is compliant with in planta experiments for agronomic studies.

Highlights

  • Global warming has increased the occurrence of stress in living plants, which forces them to adapt to the environmental conditions

  • We aim to push the boundaries of very low magnetic field nuclear magnetic resonance (NMR) by developing a highly homogenous resistive magnet while considering the constraint of self-heating, size reduction and versatility to keep the integrity of the plant under study

  • We describe an extension of the space harmonic suppression (SHS) method (Coillot et al, 2016), which allows us to enhance the magnetic field homogeneity of coils

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Summary

Introduction

Global warming has increased the occurrence of stress in living plants, which forces them to adapt to the environmental conditions. This induces some modifications in growth and composition at physiological and biochemical levels (Osakabe et al, 2014). The possibility of studying the local responses of plants to biotic and abiotic stress is limited since current anatomical and biochemical methods are destructive and do not allow us to investigate plants. The 1H NMR signal is roughly quadratically dependent on the intensity of the magnetic field (Vo-Dinh, 2002). This consideration has historically oriented the NMR spectrometer design to higher mag-

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