Abstract
A number of N-acylalkylenediamines were synthesized in high yields by in situ monoamidation of car☐ylic acids with diamines. The amidation reactions were carried out simply by heating the substrates at 110 °C for 5–24 h in the presence of HMDS. HMDS-promoted in situ amidation reactions are generally applicable to the synthesis of N-acylalkylenediamines. [Display omitted]
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