Abstract
In the presence of catalytic amount of cesium hydroxide, the hydrothiolation of alkynyl sulfides occurred at room temperature in DMF under nitrogen atmosphere to afford exclusive (Z)-1,2-diorganothio-1-alkene in excellent yields. It could provide a new and expedient way for the preparation of symmetrical and unsymmetrical (Z)-1,2-diorganolthio1-1-alkenes.
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