Abstract

The micro reacting pipe with 3D internal structure, which is a micromixer with the shape of the pipe, has shown great advantages regarding mass transfer and heat transfer. Since the fluid flow is mostly laminar at the micro-scale, which is unfavorable to the diffusion of reactants, it is important to understand the influence of the geometry of the microchannel on the fluid flow for improving the diffusion of the reactants and mixing efficiency. On the other hand, it is a convenient method to manufacture a micro reacting pipe in one piece through metal additive manufacturing without many post-processing processes. In this paper, a basis for the design of a micromixer model was provided by combining the metal additive manufacturing process constraints with computational fluid dynamics (CFD) simulation. The effects of microchannel structures on fluid flow and mixing efficiency were studied by CFD simulation whose results showed that the internal micro-structure had a significantly positive effect on the mixing efficiency. Based on the simulation results, the splitting-collision mechanism was discussed, and several design rules were obtained. Two different materials were selected for manufacturing with the laser powder bed fusion (L-PBF) technology. After applying pressure tests to evaluate the quality of the formed parts and comparing the corrosion-resistance of the two materials, one material was picked out for the industrial application. Additionally, the chemical experiment was conducted to evaluate the accuracy of the simulation. The experimental results showed that the mixing efficiency of the micro reacting pipe increased by 56.6%, and the optimal determining size of the micro reacting pipe was 0.2 mm. The study can be widely used in the design and manufacture of a micromixer, which can improve efficiency and reacting stability in this field.

Highlights

  • The micro reacting pipe is a kind of micromixer with the shape of a pipe which is a continuous flow chemical synthesis device with critical dimension from micron to millimeter

  • By reducing the critical dimension of the channel, the diffusion distance of the components reduces, and the mixing efficiency dominated by free diffusion is enhanced

  • The following formula (15) shows that the microscopic mixing time (t) of the micromixer is directly proportional to the square of the critical dimension (d) and inversely proportional to the component diffusion coefficient (D)

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Summary

Introduction

The micro reacting pipe is a kind of micromixer with the shape of a pipe which is a continuous flow chemical synthesis device with critical dimension from micron to millimeter. It is easy to monitor the chemical production by using this device, and there is no amplification effect. These characteristics greatly improve the mixing efficiency of micro reacting pipes, facilitate the stable control of various chemical reactions in industrial production, and shorten the R&D period of new products in chemical and pharmaceutical fields. Luong Jim et al, realized the effective management of extra-column effect and performed post-column backflushing with the 3D-printed

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