Abstract
We report the growth of high quality Fe excess and Co doped, Fe T x Se single crystals in nominal ratio via slow cooling method of high temperature solution growth technique and, their structural and physical properties through the X-ray diffraction, Raman spectroscopy, magnetic and transports measurements. Selective area electron diffraction (SAED) patterns and X-ray diffraction of cleavage piece confirm the growth of single crystals in ( h0l ) orientations. Observations of phonon vibration modes (A 1g and B 1g ) in Raman spectroscopy measurements mark the qualitative analysis of these single crystals. Low temperature magnetic and electrical transport studies manifest the superconducting nature of both single crystals.
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