Abstract

Accurate high temperature neutron diffraction experiments have been carried out between 800 degrees C and 1200 degrees C on polycrystalline Fe1-xO at compositions between Fe0.947O and Fe0.906O. The ratio of octahedral iron vacancies to tetrahedral iron interstitials is close to the value of 3.25 which would be expected if Koch-Cohen clusters persist in the high temperature equilibrium region.

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