Abstract
The high resolution, proton-decoupled 13C NMR spectra of several oxygenated hexalin, octalin and decalin derivatives have been obtained in solution and in the solid state (cross polarization, magic angle spinning). The results are used to deduce both the static (solid state) and dynamic (solution) conformational properties of these systems, and it is demonstrated that the solid state spectra provide information on the number of independent molecules in the crystallographic asymmetric unit.
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