Abstract
High-quality molybdenum-tungsten disulfide solid solutions, (Mo,W)S 2 , are rapidly synthesized in self-propagating, solid-state precursor reactions between (MoCl 5 -WCl 6 ) and Na 2 S. The mixed-metal dichalcogenide products can be readily reduced in a dilute hydrogen atmosphere at approximately 900 o C to the corresponding Mo-W alloys. The metal distribution in the Mo-W alloys is examined using the high-angle 123 powder X-ray reflection and can be correlated to the metal distribution in the metal dichalcogenide product
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