Abstract
The use of HP-NMR and HP-IR spectroscopy for a range of applications in homogeneous catalysis and coordination chemistry is described. A brief summary of the utility of such methods is followed by an overview of the instrumentation available for such studies. HP-NMR using sapphire tubes and modified probes, and transmission and reflectance cells for HP-IR analysis are discussed. Specific applications of these techniques to the analysis of a range of transition metal complexes under catalytic conditions are presented. This includes discussions on mechanisms and reactive intermediates for reactions such as hydroformylation, carbonylation, and hydrogenation.
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