Abstract

In this paper, the high cycle fatigue performance of solid solution state and aged Inconel 718 superalloys was studied at room temperature. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used to analyze the original structural features and fatigue deformation features of two kinds of alloys. SEM, laser scanning confocal microscopy, and electron backscatter diffraction (EBSD) were used to analyze the secondary fracture features of the fatigue fracture morphology and fatigue fracture profile. The results showed that the aging treatment significantly affected the strength and plasticity of the alloy, which in turn affected the fatigue performance of the alloy. After the aging treatment, the yield strength σs and the tensile strength σb of the Inconel 718 alloy increased by 152% and 65.9%, respectively, compared with those of the solid solution state, but the rate of elongation δ and rate of contraction in the cross-section area φ decreased by 63.7% and 52.3%, respectively. The fatigue limit of the aged state was lower than that of the solid solution state by 6.3%. The quadratic function relationship between the high cycle fatigue limit σ−1 and the tensile strength σb of the Inconel 718 superalloy at room temperature was σ−1 = σb · (0.869−3.67 × 10−4 · σb). An analysis of the fatigue fracture mechanism showed that the fatigue fractures before and after aging were all initiated in the grains oriented relatively unfavorably on the surface of the sample, with a mixture of intergranular and transgranular propagation after the transgranular propagation of several grains. The higher plasticity of the solid solution state Inconel 718 alloy resulted in a large number of slip deformation zones under high cycle fatigue loads, and the plastic deformation was relatively uniform. The lengths of the secondary fractures were as high as 120 μm, which formed the single-source plastic fatigue fracture that promoted an increase in the fatigue limit. After aging treatment, the higher strength of the Inconel 718 alloy made dislocation slip difficult under high cycle fatigue loads, and the plasticity compatible deformation capability was poor. When local dislocations slipped to the intragranular γ” phase, γ’ phase, or interfaces with nonmetallic compounds (NMCs), plugging occurred. The degree of stress concentration increased, causing the initiation of fatigue fracture; the secondary fracture was approximately 20 μm. Brittle cleavage due to multiple sources significantly reduced the fatigue limit.

Highlights

  • The Inconel 718 superalloy is a nickel-chromium-iron (Ni-Cr-Fe)-based wrought superalloy that is precipitation-hardened and was successfully developedMetals 2019, 9, 13; doi:10.3390/met9010013 www.mdpi.com/journal/metalsMetals 2019, 9, 13 by the United States in the 1950s [1]

  • In the aging treatment process, the γ” phase, which is coherent with the matrix γ phase (Ni3 Nb, body-centered tetragonal DO22 structure), and the γ’ phase, which is semicoherent with the γ phase, disperses precipitation and hinders dislocation motion, giving the Inconel 718 alloy a higher room temperature strength and allowing this alloy to maintain a comparatively high strength at high temperatures under 650 ◦ C

  • This alloy is widely used in the manufacture of turbine discs and blades for aircraft engines and other key parts and components exposed to high temperatures and fasteners not exposed to high temperatures

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Summary

Introduction

The Inconel 718 superalloy (the trademark in China is GH4169) is a nickel-chromium-iron (Ni-Cr-Fe)-based wrought superalloy that is precipitation-hardened and was successfully developedMetals 2019, 9, 13; doi:10.3390/met9010013 www.mdpi.com/journal/metalsMetals 2019, 9, 13 by the United States in the 1950s [1]. In the aging treatment process, the γ” phase, which is coherent with the matrix γ phase (Ni3 Nb, body-centered tetragonal DO22 structure), and the γ’ phase, which is semicoherent with the γ phase (face-centered cubic LI2 structure), disperses precipitation and hinders dislocation motion, giving the Inconel 718 alloy a higher room temperature strength and allowing this alloy to maintain a comparatively high strength at high temperatures under 650 ◦ C This alloy is widely used in the manufacture of turbine discs and blades for aircraft engines and other key parts and components exposed to high temperatures and fasteners not exposed to high temperatures. Fournier et al [13] found that the Inconel 718 alloy in the solution treated and aged (ST + A) state had cyclic softening while in the direct aged (DA) state [14]

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