Abstract
We report on a new experimental NMR technique for heteronuclear polarization transfer in the rotating frame which utilizes a WALTZ-16 decoupling sequence applied synchronously to both nuclear species to effect magnetization transfer among J-coupled spins. The technique increases the tolerance to Hartmann-Hahn mismatch between coupled spins and provides easily phased one-bond correlation spectra. Long-range connectivities can also be elucidated with longer mixing times.
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