Abstract
Two (1,3-dioxan-4-yl)-methanes 3 and 10 have been synthesized by standard methods. Compound 3 has a marked (9:1) tendency to populate conformer 3b as evidenced by the 3J H,H-coupling constants in the inter-ring segment. The two additional methyl substituents in 10 increase this conformational preference to > 95:5.
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