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Abstract
Heptafluoroisopropylthio group (-SCF(CF3)2) has bioactivities in insecticidal molecules, but the protocol for direct introduction of -SCF(CF3)2 is under-explored. Described here is a protocol on heptafluoroisopropylthiolation of benzyl halides with a hexafluoropropylene (HFP)/CsF/S8 system. The reaction enables the rapid construction of a range of (CF3)2CFS-containing compounds from readily available materials. This protocol may find application in the synthesis of (CF3)2CFS-containing biologically active molecules.
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