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Abstract
Adenosine reacts with tertiary cyanopropargylic alcohols under mild conditions (K2CO3, DMF, 20–25°C, 4–30h) with 100% chemo- and regioselectivity by the way of two vicinal hydroxy groups of the ribose moiety to afford (in 52–72% yield) a novel family of adenosine cyclic ketals possessing cyano and hydroxyalkyl functions.
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