Abstract
AbstractConstruction of single‐component supramolecular triangle and unprecedented spontaneous resolution of pairs of intertwined supramolecular 31‐ and 32‐double helices by the self‐assembly of achiral 2‐(iodoethynyl)pyridine and its derivatives have been achieved through intermolecular ethynyl C−I⋅⋅⋅⋅N halogen bonds in the crystalline state. Fine‐tuning of the molecular structure of the achiral monomer and choice of solvents for crystallization have a dominant effect on the resultant supramolecular architectures.
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