Abstract
A new piperazinium 4-nitrophenolate monohydrate single crystal was grown by employing the solution growth technique piperazine and 4-nitrophenol, were the source material used for the growth. The grown crystal was characterized by Single X-ray analysis and it shows that piperazinium 4-nitrophenol monohydrate crystallizes in the monoclinic space group P21/c, with cell parameters a=10.9025(4)Å, b=6.2261(3)Å, c=14.0318(5)Å, and Z=4. The lattice parameters of the substances were also determined by using powder diffraction methods. The functional groups are identified by using FTIR spectral analysis. In addition to the solving crystal structure, the grown crystals were characterized by FT NMR, Vickers microhardness and Third Harmonic Generation (THG) studies. The absorbance and the fluorescence spectra of the title compound were analyzed using UV–Vis and PL spectra. The thermo analytical properties of the crystal were studied using TG, DTG and DTA.
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