Green reduction of silver ions to silver nanoparticles using aqueous plant extracts

Ana-Alexandra Sorescu,Ioana-Raluca Suica-Bunghez,Alexandrina Nuta

doi:10.3390/iocn2020-07909

Abstract

Silver nanoparticles are used in numerous scientific fields due to their versatile properties and because their surface can be functionalized with different biological molecules. Their synthesis follows both conventional and unconventional routes and, in recent years, the methods that start from plants are constantly detaching from the hazardous, time consuming chemical methods. This paper presents the green synthesis of silver nanoparticles from St. Benedict's herb (Geum urbanum) and its corresponding aqueous extracts via two different temperature conditions: room temperature, for 24 hours with no additional stirring and 500C, for 30 minutes under a cosntant stirring of 600 rpm. Silver nanoparticles were then characterized using UV-Vis spectroscopy at well - established time intervals in the range of 250 -650 nm and FTIR spectra were recorded to show the presence of different functional groups. DLS technique was used to investigate the particle size and zeta potential was also measured to analyze the stability of the green synthesized silver nanoparticles. TEM miscroscopy revealed a spherical - shape profile of the green synthesized silver nanoparticles and optical microscopy images were also recorded. Also, the antioxidant activity was determined using the DPPH method and compared to that of the crude aqueous extracts.

Highlights

Metallic nanoparticles are at the leading edge of nanotechnology, a scientific field that in constantly and rapidly growing ever since the physicist Richard P
This paper presents the green synthesis of silver nanoparticles from St
The bioreduction of silver ions was first visually observed by a change of color of the colloidal solutions from light green to yellow-greenish whatever the temperature conditions used for the green synthesis of AgNPs and it was confirmed by the UV–Vis recordings (Table 1)

Summary

Introduction

Metallic nanoparticles are at the leading edge of nanotechnology, a scientific field that in constantly and rapidly growing ever since the physicist Richard P. A Nobel Prize laureate, first visualized it in 1959. Metallic nanoparticles can be considered a bridge between bulk materials and molecular structures and, they exhibit unique physical-chemical properties that allows their use in numerous applications [1,2]. St. Benedict’s herb (Geum urbanum) is an astringent herb, used mainly for the treatment of different problems affecting the mouth, throat and the gastro-intestinal tract. Benedict’s herb (Geum urbanum) is an astringent herb, used mainly for the treatment of different problems affecting the mouth, throat and the gastro-intestinal tract It helps heal mouth ulcers and reduces irritation of the stomach and gut

Methods

Results

Conclusion