Abstract
Highly selective CO2 electroreduction to CO (∼90% faradaic efficiency) was achieved on NiCu0.25 bimetallic nanoparticle catalysts. By combining Synchrotron based X-ray absorption and in situ Raman spectroscopy studies, we found that there is a negative correlation between the Cu content in NiCux and CO selectivity due to redistribution of the 3d electrons.
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