Abstract

AbstractThe use of methylamine to deprotect 1‐O‐acetyl protected carbohydrates has only attracted limited interest in the literature. Demonstrated here is an approach that is able to be generalized for a wide variety of carbohydrate scaffolds which results in a high yielding, simplified, practical, expedient and clean method to prepare hemiacetals from 1‐O‐acetyl protected carbohydrates.

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