Abstract
Gel and ion-exchange chromatographic techniques were applied to the separation of lower oxo acids of phosphorus, ▪ and ▪, produced by the substitution reaction between ▪ (diphosphonate) and ▪ (diphosphate). Sephadex G-25 and Bio-Rad AG1-X8 columns were used. Hydrolysis of ▪ in the process of preparative separation is also discussed.
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