Abstract
Oxidation of Cr(CO) 5 - , Mo(CO) 5 - , and W(CO) 5 - was examined in a low-pressure (∼5×10 -8 mbar) and a high-pressure external(∼3.5 mbar) environment using a Fourier-transform ion cyclotron resonance spectrometer equipped with a high-pressure external ion source. Although the oxidation chemistry displayed by the Cr and W systems was fairly similar, the Mo analogue had several unique features. In addition, remarkable differences were observed between high- and low-pressure oxidation
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