Abstract
The use of behenic acid and sebacic acid as liquid phases for the gas-liquid chromatography of C 1 to C 5 fatty acids has been described. Complete resolution of all normal and iso-acids was obtained on 122 cm columns containing sebacic acid as the liquid phase at 135°. With behenic acid as the liquid phase the separations of formic from acetic acid and isobutyric from n-butyric acid were not quite complete at 135°, however, complete separation was obtained at 115°. Both the behenic and sebacic acid columns showed satisfactory stability at 135°.
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