Abstract
A method is described for the analysis and identification of oligosaccharides obtained by acetolysis of glycoproteins. Oligosaccharides were analyzed by gas-liquid chromatography mass spectrometry under their permethylated oligosaccharide alditol form. The suitability of the spectral data to establish the position of the glycosidic bond and the monosaccharide sequence is discussed for each oligosaccharide. This method can give structural information on small glycoprotein samples.
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