Abstract
Abstract The simultaneous N-trifluoroacetylation and O-trimethylsilylation of some iminodicarboxylic acids were studied by the use of a mixture of α,α,α,α′,α′,α′-hexafluoro-N-methyldiacetamide and N,O-bis(trimethylsilyl)trifluoroacetamide, as a derivatizing reagent. The resulting N-trifluoroacetyl trimethylsilyl ester derivatives gave rather complicated mass spectra with molecular (M+) and M–15 (loss of CH3) ions upon electron impact at 20 eV.
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